Crystallography Open Database

Information card for entry 7116442

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Coordinates	7116442.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C62 H97.5 Ca N10.5 O22 Rh4
Calculated formula	C62 H79 Ca N10.5 O21.99 Rh4
Title of publication	Thyminate(2-)-bridged cyclic tetranuclear rhodium(III) complexes formed by a template of a sodium, calcium or lanthanoid ion
Authors of publication	Ayana Kashima; Mika Sakate; Hiromi Ota; Akira Fuyuhiro; Yukinari Sunatsuki; Takayoshi Suzuki
Journal of publication	Chem.Commun.
Year of publication	2015
Journal volume	51
Pages of publication	1889
a	11.3211 ± 0.0007 Å
b	18.6735 ± 0.001 Å
c	18.7302 ± 0.0008 Å
α	89.602 ± 0.002°
β	75.171 ± 0.002°
γ	87.676 ± 0.003°
Cell volume	3824.6 ± 0.4 Å³
Cell temperature	192 ± 2 K
Ambient diffraction temperature	192 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.066
Residual factor for significantly intense reflections	0.0545
Weighted residual factors for significantly intense reflections	0.1441
Weighted residual factors for all reflections included in the refinement	0.1585
Goodness-of-fit parameter for all reflections included in the refinement	1.068
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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