Crystallography Open Database

Information card for entry 7116443

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Coordinates	7116443.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C62 H83 La N12 O19 Rh4
Calculated formula	C62 H70.294 La N12 O19 Rh4
Title of publication	Thyminate(2-)-bridged cyclic tetranuclear rhodium(III) complexes formed by a template of a sodium, calcium or lanthanoid ion
Authors of publication	Ayana Kashima; Mika Sakate; Hiromi Ota; Akira Fuyuhiro; Yukinari Sunatsuki; Takayoshi Suzuki
Journal of publication	Chem.Commun.
Year of publication	2015
Journal volume	51
Pages of publication	1889
a	18.7826 ± 0.001 Å
b	19.9113 ± 0.0012 Å
c	10.6111 ± 0.0005 Å
α	90°
β	90°
γ	90°
Cell volume	3968.4 ± 0.4 Å³
Cell temperature	186 ± 2 K
Ambient diffraction temperature	186 ± 2 K
Number of distinct elements	6
Space group number	18
Hermann-Mauguin space group symbol	P 21 21 2
Hall space group symbol	P 2 2ab
Residual factor for all reflections	0.0723
Residual factor for significantly intense reflections	0.0624
Weighted residual factors for significantly intense reflections	0.174
Weighted residual factors for all reflections included in the refinement	0.1827
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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