Information card for entry 7116598

Structure parameters

• Formula: C36.5 H25 Cl3 F6 N3 O3 P Re
• Calculated formula: C36.5 H25 Cl3 F6 N3 O3 P Re
• Title of publication: enantio-Enriched CPL-active helicene‒bipyridine‒rhenium complexes
• Authors of publication: Saleh, Nidal; Srebro, Monika; Reynaldo, Thibault; Vanthuyne, Nicolas; Toupet, Loïc; Chang, Victoria Y.; Muller, Gilles; Williams, J. A. Gareth; Roussel, Christian; Autschbach, Jochen; Crassous, Jeanne
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2015
• Journal volume: 51
• Journal issue: 18
• Pages of publication: 3754 - 3757
• a: 22.7551 ± 0.0003 Å
• b: 54.882 ± 0.001 Å
• c: 11.6412 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 14538.1 ± 0.4 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 8
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0373
• Residual factor for significantly intense reflections: 0.032
• Weighted residual factors for significantly intense reflections: 0.0775
• Weighted residual factors for all reflections included in the refinement: 0.079
• Goodness-of-fit parameter for all reflections included in the refinement: 0.937
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No