Information card for entry 7118309

Structure parameters

• Formula: H120 Li12 Mn6 Na11 O198 P5 W36
• Calculated formula: Mn6 Na3.8 O177.35 P5 W36
• Title of publication: Rearrangement of {α-P2W15} to {PW6} moieties during the assembly of transition-metal-linked polyoxometalate clusters.
• Authors of publication: Martin-Sabi, Mercè; Winter, Ross Stuart; Lydon, Claire; Cameron, Jamie M.; Long, De-Liang; Cronin, Leroy
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 5
• Pages of publication: 919 - 921
• a: 14.0471 ± 0.0002 Å
• b: 21.9582 ± 0.0004 Å
• c: 30.7558 ± 0.0004 Å
• α: 87.466 ± 0.002°
• β: 88.627 ± 0.002°
• γ: 86.131 ± 0.002°
• Cell volume: 9453.6 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1203
• Residual factor for significantly intense reflections: 0.0614
• Weighted residual factors for significantly intense reflections: 0.1616
• Weighted residual factors for all reflections included in the refinement: 0.1774
• Goodness-of-fit parameter for all reflections included in the refinement: 0.963
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No