Information card for entry 7118310

Structure parameters

• Formula: H137 Li20 Mn9 Na5 O245 P8 W45
• Calculated formula: Mn9 Na2.2 O203 P7.5 W45
• Title of publication: Rearrangement of {α-P2W15} to {PW6} moieties during the assembly of transition-metal-linked polyoxometalate clusters.
• Authors of publication: Martin-Sabi, Mercè; Winter, Ross Stuart; Lydon, Claire; Cameron, Jamie M.; Long, De-Liang; Cronin, Leroy
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 5
• Pages of publication: 919 - 921
• a: 14.0535 ± 0.0008 Å
• b: 29.6184 ± 0.0016 Å
• c: 31.8218 ± 0.0016 Å
• α: 74.118 ± 0.005°
• β: 81.242 ± 0.004°
• γ: 89.716 ± 0.004°
• Cell volume: 12582 ± 1.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1857
• Residual factor for significantly intense reflections: 0.0886
• Weighted residual factors for significantly intense reflections: 0.2096
• Weighted residual factors for all reflections included in the refinement: 0.2476
• Goodness-of-fit parameter for all reflections included in the refinement: 0.882
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No