Information card for entry 7118426

Structure parameters

• Formula: C99 H152 Ge2 Si4
• Calculated formula: C98.5 H144 Ge2 Si4
• Title of publication: Dimerization of a marginally stable disilenyl germylene to tricyclic systems: evidence for reversible NHC-coordination.
• Authors of publication: Nieder, David; Yildiz, Cem B.; Jana, Anukul; Zimmer, Michael; Huch, Volker; Scheschkewitz, David
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 13
• Pages of publication: 2799 - 2802
• a: 16.3223 ± 0.0006 Å
• b: 17.6076 ± 0.0007 Å
• c: 18.3797 ± 0.0008 Å
• α: 71.478 ± 0.0019°
• β: 77.643 ± 0.0018°
• γ: 67.458 ± 0.0017°
• Cell volume: 4600.3 ± 0.3 ų
• Cell temperature: 152 ± 2 K
• Ambient diffraction temperature: 152 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0832
• Residual factor for significantly intense reflections: 0.0492
• Weighted residual factors for significantly intense reflections: 0.1197
• Weighted residual factors for all reflections included in the refinement: 0.1353
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No