Crystallography Open Database

Information card for entry 7118427

Preview

Coordinates	7118427.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C95.5 H152 Ge2 Si4
Calculated formula	C95.5 H144 Ge2 Si4
Title of publication	Dimerization of a marginally stable disilenyl germylene to tricyclic systems: evidence for reversible NHC-coordination.
Authors of publication	Nieder, David; Yildiz, Cem B.; Jana, Anukul; Zimmer, Michael; Huch, Volker; Scheschkewitz, David
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	13
Pages of publication	2799 - 2802
a	33.8499 ± 0.0014 Å
b	26.2285 ± 0.0014 Å
c	20.2919 ± 0.0008 Å
α	90°
β	97.911 ± 0.002°
γ	90°
Cell volume	17844.3 ± 1.4 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0883
Residual factor for significantly intense reflections	0.0462
Weighted residual factors for significantly intense reflections	0.095
Weighted residual factors for all reflections included in the refinement	0.1105
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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