Information card for entry 7118819

Structure parameters

• Formula: C25 H41 Fe N2 O4 P Si3
• Calculated formula: C25 H41 Fe N2 O4 P Si3
• Title of publication: Phosphinosilylenes as a novel ligand system for heterobimetallic complexes.
• Authors of publication: Breit, Nora C.; Eisenhut, Carsten; Inoue, Shigeyoshi
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 32
• Pages of publication: 5523 - 5526
• a: 11.1641 ± 0.0001 Å
• b: 16.6308 ± 0.0001 Å
• c: 17.5587 ± 0.0001 Å
• α: 90°
• β: 94.787 ± 0.001°
• γ: 90°
• Cell volume: 3248.72 ± 0.04 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0338
• Residual factor for significantly intense reflections: 0.0304
• Weighted residual factors for significantly intense reflections: 0.0789
• Weighted residual factors for all reflections included in the refinement: 0.081
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No