Crystallography Open Database

Information card for entry 7118820

Preview

Coordinates	7118820.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53 H62 Fe2 N4 O18 P2 Si2 W2
Calculated formula	C53 H62 Fe2 N4 O18 P2 Si2 W2
Title of publication	Phosphinosilylenes as a novel ligand system for heterobimetallic complexes.
Authors of publication	Breit, Nora C.; Eisenhut, Carsten; Inoue, Shigeyoshi
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	32
Pages of publication	5523 - 5526
a	25.6547 ± 0.0002 Å
b	10.4018 ± 0.0001 Å
c	24.8836 ± 0.0002 Å
α	90°
β	91.797 ± 0.001°
γ	90°
Cell volume	6637.05 ± 0.1 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0334
Residual factor for significantly intense reflections	0.031
Weighted residual factors for significantly intense reflections	0.0803
Weighted residual factors for all reflections included in the refinement	0.0827
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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