Information card for entry 7119687

Structure parameters

• Formula: C17 H19 N O7
• Calculated formula: C17 H19 N O7
• SMILES: N1C(=O)c2cc3OCOc3cc2[C@H]2[C@H](O)[C@H](O)[C@H]3OC(O[C@H]3[C@H]12)(C)C
• Title of publication: Asymmetric cinnamylation of N-tert-butanesulfinyl imines with cinnamyl acetates: total syntheses of (+)-lycoricidine and (+)-7-deoxypancratistatin.
• Authors of publication: Cai, Sen-Lin; Yuan, Bin-Hua; Jiang, Yi-Xiang; Lin, Guo-Qiang; Sun, Xing-Wen
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2017
• Journal volume: 53
• Journal issue: 25
• Pages of publication: 3520 - 3523
• a: 19.5766 ± 0.0015 Å
• b: 8.3899 ± 0.0007 Å
• c: 9.3442 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1534.7 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0321
• Residual factor for significantly intense reflections: 0.0303
• Weighted residual factors for significantly intense reflections: 0.0836
• Weighted residual factors for all reflections included in the refinement: 0.0848
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No