Crystallography Open Database

Information card for entry 7119688

7119687 << 7119688 >> 7119689

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Coordinates	7119688.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C114 H108 Dy8 N48 O42
Calculated formula	C114 H108 Dy8 N48 O42
Title of publication	End-to-end azido-pinned interlocking lanthanide squares.
Authors of publication	Li, Xiao-Lei; Wu, Jianfeng; Zhao, Lang; Shi, Wei; Cheng, Peng; Tang, Jinkui
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2017
Journal volume	53
Journal issue	21
Pages of publication	3026 - 3029
a	22.7096 ± 0.001 Å
b	30.714 ± 0.0012 Å
c	52.896 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	36895 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	70
Hermann-Mauguin space group symbol	F d d d
Hall space group symbol	-F 2uv 2vw
Residual factor for all reflections	0.0789
Residual factor for significantly intense reflections	0.0604
Weighted residual factors for significantly intense reflections	0.1952
Weighted residual factors for all reflections included in the refinement	0.2257
Goodness-of-fit parameter for all reflections included in the refinement	1.005
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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