Crystallography Open Database

Information card for entry 7119712

7119711 << 7119712 >> 7119713

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Coordinates	7119712.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H38 F3 N2 O3 S Sn
Calculated formula	C31 H38 F3 N2 O3 S Sn
Title of publication	Reactivity of heavy carbene analogues towards oxidants: a redox active ligand-enabled isolation of a paramagnetic stannylene.
Authors of publication	Janes, Trevor; Zatsepin, Pavel; Song, Datong
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2017
Journal volume	53
Journal issue	21
Pages of publication	3090 - 3093
a	30.2756 ± 0.0012 Å
b	11.6808 ± 0.0005 Å
c	17.9498 ± 0.0007 Å
α	90°
β	94.9769 ± 0.0018°
γ	90°
Cell volume	6323.9 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0497
Residual factor for significantly intense reflections	0.032
Weighted residual factors for significantly intense reflections	0.0634
Weighted residual factors for all reflections included in the refinement	0.0697
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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