Information card for entry 7119713

Structure parameters

• Formula: C30 H38 N2 Pb
• Calculated formula: C30 H38 N2 Pb
• Title of publication: Reactivity of heavy carbene analogues towards oxidants: a redox active ligand-enabled isolation of a paramagnetic stannylene.
• Authors of publication: Janes, Trevor; Zatsepin, Pavel; Song, Datong
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2017
• Journal volume: 53
• Journal issue: 21
• Pages of publication: 3090 - 3093
• a: 10.9016 ± 0.0007 Å
• b: 21.6336 ± 0.0017 Å
• c: 11.6083 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2737.7 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0429
• Residual factor for significantly intense reflections: 0.0275
• Weighted residual factors for significantly intense reflections: 0.0571
• Weighted residual factors for all reflections included in the refinement: 0.0614
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No