Information card for entry 7120774

Structure parameters

• Formula: C72 H162 Ce2 O24 Si6
• Calculated formula: C72 H162 Ce2 O24 Si6
• Title of publication: Synthesis and derivatisation of ceric tris(tert-butoxy)siloxides
• Authors of publication: Friedrich, Jochen; Maichle-moessmer, Caecilia; Anwander, Reiner
• Journal of publication: Chem. Commun.
• Year of publication: 2017
• a: 26.0279 ± 0.001 Å
• b: 14.1706 ± 0.0005 Å
• c: 27.354 ± 0.001 Å
• α: 90°
• β: 97.351 ± 0.002°
• γ: 90°
• Cell volume: 10006.1 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0664
• Residual factor for significantly intense reflections: 0.0453
• Weighted residual factors for significantly intense reflections: 0.0833
• Weighted residual factors for all reflections included in the refinement: 0.0895
• Goodness-of-fit parameter for all reflections included in the refinement: 1.145
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No