Information card for entry 7120775

Structure parameters

• Formula: C53 H123 Ce O16 Si5 Zn
• Calculated formula: C53 H123 Ce O16 Si5 Zn
• Title of publication: Synthesis and derivatisation of ceric tris(tert-butoxy)siloxides
• Authors of publication: Friedrich, Jochen; Maichle-moessmer, Caecilia; Anwander, Reiner
• Journal of publication: Chem. Commun.
• Year of publication: 2017
• a: 19.3644 ± 0.0015 Å
• b: 20.0689 ± 0.0016 Å
• c: 20.9286 ± 0.0018 Å
• α: 90°
• β: 111.894 ± 0.003°
• γ: 90°
• Cell volume: 7546.7 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0367
• Residual factor for significantly intense reflections: 0.0279
• Weighted residual factors for significantly intense reflections: 0.0622
• Weighted residual factors for all reflections included in the refinement: 0.0665
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No