Information card for entry 7120777

Structure parameters

• Formula: C47 H104 Ce O15.5 Si3
• Calculated formula: C47 H104 Ce O15.5 Si3
• Title of publication: Synthesis and derivatisation of ceric tris(tert-butoxy)siloxides
• Authors of publication: Friedrich, Jochen; Maichle-moessmer, Caecilia; Anwander, Reiner
• Journal of publication: Chem. Commun.
• Year of publication: 2017
• a: 46.814 ± 0.003 Å
• b: 13.9872 ± 0.0009 Å
• c: 19.116 ± 0.0012 Å
• α: 90°
• β: 99.748 ± 0.002°
• γ: 90°
• Cell volume: 12336.4 ± 1.4 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0373
• Residual factor for significantly intense reflections: 0.0296
• Weighted residual factors for significantly intense reflections: 0.0674
• Weighted residual factors for all reflections included in the refinement: 0.0712
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No