Information card for entry 7120776

Structure parameters

• Formula: C48 H108 Ce Cl O16 Si4 Zn
• Calculated formula: C48 H108 Ce Cl O16 Si4 Zn
• Title of publication: Synthesis and derivatisation of ceric tris(tert-butoxy)siloxides
• Authors of publication: Friedrich, Jochen; Maichle-moessmer, Caecilia; Anwander, Reiner
• Journal of publication: Chem. Commun.
• Year of publication: 2017
• a: 13.237 ± 0.002 Å
• b: 20.065 ± 0.004 Å
• c: 28.704 ± 0.005 Å
• α: 90°
• β: 90.639 ± 0.01°
• γ: 90°
• Cell volume: 7623 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0959
• Residual factor for significantly intense reflections: 0.0557
• Weighted residual factors for significantly intense reflections: 0.1365
• Weighted residual factors for all reflections included in the refinement: 0.1512
• Goodness-of-fit parameter for all reflections included in the refinement: 0.983
• Diffraction radiation wavelength: 0.71073 Å
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No