Crystallography Open Database

Information card for entry 7121070

Preview

Coordinates	7121070.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H15 F10 Rh
Calculated formula	C22 H15 F10 Rh
Title of publication	Hidden aryl-exchange processes in stable 16e Rh<sup>III</sup> [RhCp*Ar<sub>2</sub>] complexes, and their unexpected transmetalation mechanism.
Authors of publication	Peñas-Defrutos, M N; Bartolomé, C; García-Melchor, M; Espinet, P.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	8
Pages of publication	984 - 987
a	12.1906 ± 0.0002 Å
b	18.7742 ± 0.0003 Å
c	9.17539 ± 0.00017 Å
α	90°
β	90°
γ	90°
Cell volume	2099.96 ± 0.06 Å³
Cell temperature	294 K
Ambient diffraction temperature	294 K
Number of distinct elements	4
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0536
Residual factor for significantly intense reflections	0.0449
Weighted residual factors for significantly intense reflections	0.116
Weighted residual factors for all reflections included in the refinement	0.1249
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7121070.html