Information card for entry 7121869

Structure parameters

• Formula: C18 H32 I N4 P
• Calculated formula: C18 H32 I N4 P
• Title of publication: Isolable N-heterocyclic carbene adducts of the elusive diiodophosphine.
• Authors of publication: Cicač-Hudi, M; Schlindwein, S. H.; Feil, C. M.; Nieger, M.; Gudat, D.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 55
• Pages of publication: 7645 - 7648
• a: 9.4547 ± 0.0006 Å
• b: 19.5345 ± 0.0012 Å
• c: 11.8695 ± 0.0007 Å
• α: 90°
• β: 94.891 ± 0.003°
• γ: 90°
• Cell volume: 2184.2 ± 0.2 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0305
• Residual factor for significantly intense reflections: 0.0243
• Weighted residual factors for significantly intense reflections: 0.0574
• Weighted residual factors for all reflections included in the refinement: 0.0608
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No