Information card for entry 7121870

Structure parameters

• Formula: C9 H17 I2 N2 P
• Calculated formula: C9 H17 I2 N2 P
• Title of publication: Isolable N-heterocyclic carbene adducts of the elusive diiodophosphine.
• Authors of publication: Cicač-Hudi, M; Schlindwein, S. H.; Feil, C. M.; Nieger, M.; Gudat, D.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 55
• Pages of publication: 7645 - 7648
• a: 7.7774 ± 0.0005 Å
• b: 8.4078 ± 0.0006 Å
• c: 11.6208 ± 0.0008 Å
• α: 84.753 ± 0.004°
• β: 79.435 ± 0.003°
• γ: 78.409 ± 0.003°
• Cell volume: 730.6 ± 0.09 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0268
• Residual factor for significantly intense reflections: 0.0214
• Weighted residual factors for significantly intense reflections: 0.0491
• Weighted residual factors for all reflections included in the refinement: 0.0525
• Goodness-of-fit parameter for all reflections included in the refinement: 1.243
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No