Information card for entry 7121956

Structure parameters

• Formula: C84 H112 O6 Sm4
• Calculated formula: C84 H112 O6 Sm4
• Title of publication: Synthesis of homometallic divalent lanthanide organoimides from benzyl complexes.
• Authors of publication: Wolf, Benjamin M.; Stuhl, Christoph; Anwander, Reiner
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 64
• Pages of publication: 8826 - 8829
• a: 12.252 ± 0.006 Å
• b: 12.49 ± 0.008 Å
• c: 12.826 ± 0.005 Å
• α: 84.442 ± 0.017°
• β: 77.873 ± 0.01°
• γ: 80.73 ± 0.06°
• Cell volume: 1889.8 ± 1.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0391
• Residual factor for significantly intense reflections: 0.0265
• Weighted residual factors for significantly intense reflections: 0.0541
• Weighted residual factors for all reflections included in the refinement: 0.0593
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No