Information card for entry 7121957

Structure parameters

• Formula: C22 H34 O4 Yb
• Calculated formula: C22 H34 O4 Yb
• Title of publication: Synthesis of homometallic divalent lanthanide organoimides from benzyl complexes.
• Authors of publication: Wolf, Benjamin M.; Stuhl, Christoph; Anwander, Reiner
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 64
• Pages of publication: 8826 - 8829
• a: 13.172 ± 0.011 Å
• b: 12.265 ± 0.005 Å
• c: 14.497 ± 0.007 Å
• α: 90°
• β: 90.35 ± 0.04°
• γ: 90°
• Cell volume: 2342 ± 2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0187
• Residual factor for significantly intense reflections: 0.0156
• Weighted residual factors for significantly intense reflections: 0.0382
• Weighted residual factors for all reflections included in the refinement: 0.0397
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No