Crystallography Open Database

Information card for entry 7122259

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Coordinates	7122259.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H31 N O P2
Calculated formula	C34 H31 N O P2
Title of publication	1,1-Diphosphines and divinylphosphines via base catalyzed hydrophosphination.
Authors of publication	Coles, N. T.; Mahon, M. F.; Webster, R. L.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	74
Pages of publication	10443 - 10446
a	17.0617 ± 0.0003 Å
b	10.7421 ± 0.0001 Å
c	17.4615 ± 0.0003 Å
α	90°
β	117.433 ± 0.002°
γ	90°
Cell volume	2840.44 ± 0.09 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	5
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0231
Residual factor for significantly intense reflections	0.023
Weighted residual factors for significantly intense reflections	0.0616
Weighted residual factors for all reflections included in the refinement	0.0618
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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