Information card for entry 7122260

Structure parameters

• Formula: C41 H36 N2 P2
• Calculated formula: C41 H36 N2 P2
• Title of publication: 1,1-Diphosphines and divinylphosphines via base catalyzed hydrophosphination.
• Authors of publication: Coles, N. T.; Mahon, M. F.; Webster, R. L.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 74
• Pages of publication: 10443 - 10446
• a: 10.1534 ± 0.0003 Å
• b: 18.1256 ± 0.0004 Å
• c: 18.7968 ± 0.0005 Å
• α: 90°
• β: 99.266 ± 0.003°
• γ: 90°
• Cell volume: 3414.16 ± 0.16 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.061
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for significantly intense reflections: 0.1033
• Weighted residual factors for all reflections included in the refinement: 0.1127
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No