Crystallography Open Database

Information card for entry 7122348

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Coordinates	7122348.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H49 B9 N2 O
Calculated formula	C29 H49 B9 N2 O
Title of publication	Rhodium(iii)-catalyzed dehydrogenative dialkenylation of the monocarba-closo-decaborate cluster by regioselective B-H activation.
Authors of publication	Liang, Xuewei; Shen, Yunjun; Zhang, Kang; Liu, Jiyong; Duttwyler, Simon
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	88
Pages of publication	12451 - 12454
a	7.9588 ± 0.0002 Å
b	22.66 ± 0.0004 Å
c	18.5609 ± 0.0003 Å
α	90°
β	90.433 ± 0.001°
γ	90°
Cell volume	3347.3 ± 0.12 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 K
Number of distinct elements	5
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0341
Residual factor for significantly intense reflections	0.0333
Weighted residual factors for significantly intense reflections	0.085
Weighted residual factors for all reflections included in the refinement	0.0857
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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