Information card for entry 7122349

Structure parameters

• Formula: C11 H25 B9 N Na O5 S2
• Calculated formula: C11 H25 B9 N Na O5 S2
• Title of publication: Rhodium(iii)-catalyzed dehydrogenative dialkenylation of the monocarba-closo-decaborate cluster by regioselective B-H activation.
• Authors of publication: Liang, Xuewei; Shen, Yunjun; Zhang, Kang; Liu, Jiyong; Duttwyler, Simon
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 88
• Pages of publication: 12451 - 12454
• a: 14.3755 ± 0.0008 Å
• b: 11.2861 ± 0.0006 Å
• c: 51.571 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8367.1 ± 0.8 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1897
• Residual factor for significantly intense reflections: 0.165
• Weighted residual factors for significantly intense reflections: 0.3796
• Weighted residual factors for all reflections included in the refinement: 0.3961
• Goodness-of-fit parameter for all reflections included in the refinement: 0.924
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No