Information card for entry 7122768

Structure parameters

• Chemical name: Ge
• Formula: C26 H28 Ge
• Calculated formula: C26 H28 Ge
• Title of publication: Synthesis of carbonyl-bridged dibenzofulvalenes and related compounds by rhodium-catalyzed stitching reaction.
• Authors of publication: Shintani, Ryo; Kishikawa, Shinnosuke; Nakamura, Kimihiro; Tsuda, Tomohiro; Nozaki, Kyoko
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2019
• a: 16.8701 ± 0.0006 Å
• b: 16.9405 ± 0.0006 Å
• c: 18.3624 ± 0.0003 Å
• α: 100.752 ± 0.002°
• β: 100.803 ± 0.002°
• γ: 119.398 ± 0.004°
• Cell volume: 4246.4 ± 0.3 ų
• Cell temperature: 113 K
• Ambient diffraction temperature: 113 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.0297
• Weighted residual factors for significantly intense reflections: 0.063
• Weighted residual factors for all reflections included in the refinement: 0.0648
• Goodness-of-fit parameter for all reflections included in the refinement: 0.979
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No