Information card for entry 7122769

Structure parameters

• Formula: C30 H38 O2 S Si2
• Calculated formula: C30 H38 O2 S Si2
• Title of publication: Synthesis of carbonyl-bridged dibenzofulvalenes and related compounds by rhodium-catalyzed stitching reaction.
• Authors of publication: Shintani, Ryo; Kishikawa, Shinnosuke; Nakamura, Kimihiro; Tsuda, Tomohiro; Nozaki, Kyoko
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2019
• a: 10.249 ± 0.002 Å
• b: 11.586 ± 0.003 Å
• c: 12.434 ± 0.003 Å
• α: 82.379 ± 0.009°
• β: 77.407 ± 0.008°
• γ: 85.599 ± 0.008°
• Cell volume: 1426.5 ± 0.6 ų
• Cell temperature: 93 K
• Ambient diffraction temperature: 93 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0372
• Residual factor for significantly intense reflections: 0.0357
• Weighted residual factors for significantly intense reflections: 0.0874
• Weighted residual factors for all reflections included in the refinement: 0.0884
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No