Information card for entry 7122770

Structure parameters

• Formula: C36 H43 O P Si2
• Calculated formula: C36 H43 O P Si2
• Title of publication: Synthesis of carbonyl-bridged dibenzofulvalenes and related compounds by rhodium-catalyzed stitching reaction.
• Authors of publication: Shintani, Ryo; Kishikawa, Shinnosuke; Nakamura, Kimihiro; Tsuda, Tomohiro; Nozaki, Kyoko
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2019
• a: 15.237 ± 0.004 Å
• b: 10.387 ± 0.003 Å
• c: 20.841 ± 0.005 Å
• α: 90°
• β: 107.636 ± 0.003°
• γ: 90°
• Cell volume: 3143.4 ± 1.4 ų
• Cell temperature: 93 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0559
• Residual factor for significantly intense reflections: 0.0454
• Weighted residual factors for significantly intense reflections: 0.1024
• Weighted residual factors for all reflections included in the refinement: 0.1092
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No