Crystallography Open Database

Information card for entry 7122863

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Structure parameters

Formula	C34 H17 B F15 P Si
Calculated formula	C34 H17 B F15 P Si
Title of publication	A self-hydrosilylation of phosphanylhydrosilylalkynes promoted by B(C6F5)3? An experimental and mechanistic study
Authors of publication	Huang, Yanting; Wang, Xiaoping; Li, Yan; Yang, Ming-Chung; Su, Ming-Der; Zhu, Hongping
Journal of publication	Chemical Communications
Year of publication	2019
a	9.9289 ± 0.0005 Å
b	12.0268 ± 0.0006 Å
c	14.753 ± 0.0007 Å
α	76.372 ± 0.004°
β	79.509 ± 0.004°
γ	69.177 ± 0.005°
Cell volume	1590.87 ± 0.15 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0482
Residual factor for significantly intense reflections	0.0391
Weighted residual factors for significantly intense reflections	0.0823
Weighted residual factors for all reflections included in the refinement	0.0864
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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