Information card for entry 7122864

Structure parameters

• Formula: C36 H21 B F15 P Si
• Calculated formula: C36 H21 B F15 P Si
• Title of publication: A self-hydrosilylation of phosphanylhydrosilylalkynes promoted by B(C6F5)3? An experimental and mechanistic study
• Authors of publication: Huang, Yanting; Wang, Xiaoping; Li, Yan; Yang, Ming-Chung; Su, Ming-Der; Zhu, Hongping
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 11.5534 ± 0.0004 Å
• b: 11.9538 ± 0.0005 Å
• c: 13.8924 ± 0.0003 Å
• α: 88.901 ± 0.002°
• β: 73.743 ± 0.003°
• γ: 69.443 ± 0.004°
• Cell volume: 1717.94 ± 0.12 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0657
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for significantly intense reflections: 0.1837
• Weighted residual factors for all reflections included in the refinement: 0.1905
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No