Information card for entry 7122865

Structure parameters

• Formula: C37.25 H22.25 B Cl3.75 F15 P Si
• Calculated formula: C37.25 H22.25 B Cl3.75 F15 P Si
• Title of publication: A self-hydrosilylation of phosphanylhydrosilylalkynes promoted by B(C6F5)3? An experimental and mechanistic study
• Authors of publication: Huang, Yanting; Wang, Xiaoping; Li, Yan; Yang, Ming-Chung; Su, Ming-Der; Zhu, Hongping
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 35.6477 ± 0.0003 Å
• b: 36.903 ± 0.0003 Å
• c: 12.0968 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 15913.4 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0435
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1232
• Weighted residual factors for all reflections included in the refinement: 0.1242
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No