Information card for entry 7123369

Structure parameters

• Formula: C69.5 H90 Mn N4 O6 Yb
• Calculated formula: C69.5 H90 Mn N4 O6 Yb
• Title of publication: Rhenium is different: CO tetramerization induced by a divalent lanthanide complex in rhenium carbonyls
• Authors of publication: Yadav, Ravi; Simler, Thomas; Gamer, Michael T.; Köppe, Ralf; Roesky, Peter W.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 12.1458 ± 0.0006 Å
• b: 13.5433 ± 0.0007 Å
• c: 19.7641 ± 0.001 Å
• α: 90.345 ± 0.004°
• β: 96.876 ± 0.004°
• γ: 98.184 ± 0.004°
• Cell volume: 3193.9 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.04
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for significantly intense reflections: 0.0665
• Weighted residual factors for all reflections included in the refinement: 0.0697
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No