Information card for entry 7123370

Structure parameters

• Formula: C128 H176 Mn4 O27 Sm4
• Calculated formula: C128 H176 Mn4 O27 Sm4
• Title of publication: Rhenium is different: CO tetramerization induced by a divalent lanthanide complex in rhenium carbonyls
• Authors of publication: Yadav, Ravi; Simler, Thomas; Gamer, Michael T.; Köppe, Ralf; Roesky, Peter W.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 12.6229 ± 0.0004 Å
• b: 12.8766 ± 0.0004 Å
• c: 20.642 ± 0.0007 Å
• α: 101.808 ± 0.003°
• β: 94.242 ± 0.003°
• γ: 90.676 ± 0.003°
• Cell volume: 3273.91 ± 0.19 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0806
• Residual factor for significantly intense reflections: 0.0446
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.1084
• Goodness-of-fit parameter for all reflections included in the refinement: 0.953
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No