Aluminium-catalysed isocyanate trimerization, enhanced by exploiting a dynamic coordination sphere
Authors of publication
Bahili, Mohammed A.; Stokes, Emily C.; Amesbury, Robert C.; Ould, Darren M. C.; Christo, Bashar; Horne, Rhian J.; Kariuki, Benson M.; Stewart, Jack A.; Taylor, Rebekah L.; Williams, P. Andrew; Jones, Matthew D.; Harris, Kenneth D. M.; Ward, Benjamin D.
Journal of publication
Chemical Communications
Year of publication
2019
a
13.1448 ± 0.0005 Å
b
13.1448 ± 0.0005 Å
c
26.2723 ± 0.0011 Å
α
90°
β
90°
γ
120°
Cell volume
3931.3 ± 0.3 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
4
Space group number
161
Hermann-Mauguin space group symbol
R 3 c :H
Hall space group symbol
R 3 -2"c
Residual factor for all reflections
0.0472
Residual factor for significantly intense reflections
0.0428
Weighted residual factors for significantly intense reflections
0.1304
Weighted residual factors for all reflections included in the refinement
0.1346
Goodness-of-fit parameter for all reflections included in the refinement
