Aluminium-catalysed isocyanate trimerization, enhanced by exploiting a dynamic coordination sphere
Authors of publication
Bahili, Mohammed A.; Stokes, Emily C.; Amesbury, Robert C.; Ould, Darren M. C.; Christo, Bashar; Horne, Rhian J.; Kariuki, Benson M.; Stewart, Jack A.; Taylor, Rebekah L.; Williams, P. Andrew; Jones, Matthew D.; Harris, Kenneth D. M.; Ward, Benjamin D.
Journal of publication
Chemical Communications
Year of publication
2019
a
7.3989 ± 0.0003 Å
b
5.9654 ± 0.0004 Å
c
31.516 ± 0.0016 Å
α
90°
β
90°
γ
90°
Cell volume
1391.03 ± 0.13 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
4
Space group number
61
Hermann-Mauguin space group symbol
P b c a
Hall space group symbol
-P 2ac 2ab
Residual factor for all reflections
0.0707
Residual factor for significantly intense reflections
0.0519
Weighted residual factors for significantly intense reflections
0.1226
Weighted residual factors for all reflections included in the refinement
0.1347
Goodness-of-fit parameter for all reflections included in the refinement
