Aluminium-catalysed isocyanate trimerization, enhanced by exploiting a dynamic coordination sphere
Authors of publication
Bahili, Mohammed A.; Stokes, Emily C.; Amesbury, Robert C.; Ould, Darren M. C.; Christo, Bashar; Horne, Rhian J.; Kariuki, Benson M.; Stewart, Jack A.; Taylor, Rebekah L.; Williams, P. Andrew; Jones, Matthew D.; Harris, Kenneth D. M.; Ward, Benjamin D.
Journal of publication
Chemical Communications
Year of publication
2019
a
12.6283 ± 0.0003 Å
b
12.6283 ± 0.0003 Å
c
26.611 ± 0.001 Å
α
90°
β
90°
γ
120°
Cell volume
3675.21 ± 0.19 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
4
Space group number
161
Hermann-Mauguin space group symbol
R 3 c :H
Hall space group symbol
R 3 -2"c
Residual factor for all reflections
0.0374
Residual factor for significantly intense reflections
0.0358
Weighted residual factors for significantly intense reflections
0.0957
Weighted residual factors for all reflections included in the refinement
0.0971
Goodness-of-fit parameter for all reflections included in the refinement
