Information card for entry 7124214

Structure parameters

• Formula: C120 H270 Cl2 Si10 Sn20
• Calculated formula: C120 H270 Cl2 Si10 Sn20
• Title of publication: Sn20(SitBu3)10Cl2 ‒ the largest metalloid group 14 cluster shows a raspberry-like arrangement of smaller units
• Authors of publication: Schnepf, Andreas; Schrenk, Claudio; Binder, Mareike
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 19.176 ± 0.004 Å
• b: 23.573 ± 0.005 Å
• c: 20.419 ± 0.004 Å
• α: 90°
• β: 92.82 ± 0.004°
• γ: 90°
• Cell volume: 9219 ± 3 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1368
• Residual factor for significantly intense reflections: 0.0708
• Weighted residual factors for significantly intense reflections: 0.1513
• Weighted residual factors for all reflections included in the refinement: 0.1901
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No