Information card for entry 7124622

Structure parameters

• Formula: C38 H49 N3 Nb
• Calculated formula: C38 H49 N3 Nb
• Title of publication: Photo-activation of d(0) niobium imido azides: en route to nitrido complexes.
• Authors of publication: Camp, Clément; Grant, Lauren N.; Bergman, Robert G.; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 32
• Pages of publication: 5538 - 5541
• a: 12.4801 ± 0.0005 Å
• b: 13.772 ± 0.0005 Å
• c: 19.2824 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3314.2 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 58
• Hermann-Mauguin space group symbol: P n n m
• Hall space group symbol: -P 2 2n
• Residual factor for all reflections: 0.0426
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.0969
• Weighted residual factors for all reflections included in the refinement: 0.0988
• Goodness-of-fit parameter for all reflections included in the refinement: 1.097
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No