Information card for entry 7124623

Structure parameters

• Formula: C67 H72 B F15 N5 Nb
• Calculated formula: C67 H72 B F15 N5 Nb
• Title of publication: Photo-activation of d(0) niobium imido azides: en route to nitrido complexes.
• Authors of publication: Camp, Clément; Grant, Lauren N.; Bergman, Robert G.; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 32
• Pages of publication: 5538 - 5541
• a: 12.5396 ± 0.0009 Å
• b: 17.4757 ± 0.0011 Å
• c: 29.99 ± 0.002 Å
• α: 84.127 ± 0.003°
• β: 82.987 ± 0.003°
• γ: 73.602 ± 0.003°
• Cell volume: 6241.6 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1424
• Residual factor for significantly intense reflections: 0.0799
• Weighted residual factors for significantly intense reflections: 0.1818
• Weighted residual factors for all reflections included in the refinement: 0.2127
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No