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Information card for entry 7124682
Preview
Coordinates | 7124682.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C66 H57 Ce F15 N3 O2 P2 S6 Si3 |
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Calculated formula | C66 H57 Ce F15 N3 O2 P2 S6 Si3 |
Title of publication | Reactions of a cerium(iii) amide with heteroallenes: insertion, silyl-migration and de-insertion. |
Authors of publication | Yin, Haolin; Carroll, Patrick J.; Schelter, Eric J. |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2016 |
Journal volume | 52 |
Journal issue | 63 |
Pages of publication | 9813 - 9816 |
a | 13.5981 ± 0.0006 Å |
b | 14.8764 ± 0.0007 Å |
c | 21.2531 ± 0.0009 Å |
α | 75.799 ± 0.002° |
β | 87.413 ± 0.002° |
γ | 75.372 ± 0.002° |
Cell volume | 4032.2 ± 0.3 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 ± 1 K |
Number of distinct elements | 9 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0623 |
Residual factor for significantly intense reflections | 0.0511 |
Weighted residual factors for significantly intense reflections | 0.1185 |
Weighted residual factors for all reflections included in the refinement | 0.1253 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.096 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7124682.html
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