Information card for entry 7124796

Structure parameters

• Formula: C14 H23 O6 P Si2 W
• Calculated formula: C14 H23 O6 P Si2 W
• Title of publication: A novel route to C-unsubstituted 1,2-oxaphosphetane and 1,2-oxaphospholane complexes.
• Authors of publication: Kyri, A. W.; Schnakenburg, G.; Streubel, R.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 55
• Pages of publication: 8593 - 8595
• a: 9.7786 ± 0.0005 Å
• b: 9.9521 ± 0.0004 Å
• c: 21.9977 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2140.76 ± 0.17 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0244
• Residual factor for significantly intense reflections: 0.0221
• Weighted residual factors for significantly intense reflections: 0.0369
• Weighted residual factors for all reflections included in the refinement: 0.0376
• Goodness-of-fit parameter for all reflections included in the refinement: 0.886
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No