Information card for entry 7124797

Structure parameters

• Chemical name: AKY-424
• Formula: C14 H24 I O6 P Si2 W
• Calculated formula: C14 H24 I O6 P Si2 W
• Title of publication: A novel route to C-unsubstituted 1,2-oxaphosphetane and 1,2-oxaphospholane complexes.
• Authors of publication: Kyri, A. W.; Schnakenburg, G.; Streubel, R.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 55
• Pages of publication: 8593 - 8595
• a: 9.179 ± 0.003 Å
• b: 10.433 ± 0.004 Å
• c: 14.066 ± 0.005 Å
• α: 86.293 ± 0.01°
• β: 81.81 ± 0.01°
• γ: 65.584 ± 0.009°
• Cell volume: 1214 ± 0.8 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1918
• Residual factor for significantly intense reflections: 0.1405
• Weighted residual factors for significantly intense reflections: 0.3049
• Weighted residual factors for all reflections included in the refinement: 0.3359
• Goodness-of-fit parameter for all reflections included in the refinement: 1.231
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No