Information card for entry 7125172

Structure parameters

• Formula: C14 H24 O P2 S2
• Calculated formula: C14 H24 O P2 S2
• Title of publication: Rhodium-catalyzed P-P bond exchange reaction of diphosphine disulfides.
• Authors of publication: Arisawa, Mieko; Yamada, Tomoki; Tanii, Saori; Kawada, Yuta; Hashimoto, Hisako; Yamaguchi, Masahiko
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 93
• Pages of publication: 13580 - 13583
• a: 6.4559 ± 0.0004 Å
• b: 12.3783 ± 0.0006 Å
• c: 22.5131 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1799.09 ± 0.18 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1078
• Residual factor for significantly intense reflections: 0.0606
• Weighted residual factors for significantly intense reflections: 0.1067
• Weighted residual factors for all reflections included in the refinement: 0.1536
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No