Information card for entry 7125173

Structure parameters

• Formula: C16 H20 P2 S2
• Calculated formula: C16 H20 P2 S2
• Title of publication: Rhodium-catalyzed P-P bond exchange reaction of diphosphine disulfides.
• Authors of publication: Arisawa, Mieko; Yamada, Tomoki; Tanii, Saori; Kawada, Yuta; Hashimoto, Hisako; Yamaguchi, Masahiko
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 93
• Pages of publication: 13580 - 13583
• a: 9.3474 ± 0.0007 Å
• b: 7.1672 ± 0.0004 Å
• c: 13.3103 ± 0.0008 Å
• α: 90°
• β: 101.49 ± 0.002°
• γ: 90°
• Cell volume: 873.85 ± 0.1 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0498
• Residual factor for significantly intense reflections: 0.0391
• Weighted residual factors for significantly intense reflections: 0.0964
• Weighted residual factors for all reflections included in the refinement: 0.1213
• Goodness-of-fit parameter for all reflections included in the refinement: 1.268
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No