Information card for entry 7125174

Structure parameters

• Formula: C15 H18 P2 S2
• Calculated formula: C15 H18 P2 S2
• Title of publication: Rhodium-catalyzed P-P bond exchange reaction of diphosphine disulfides.
• Authors of publication: Arisawa, Mieko; Yamada, Tomoki; Tanii, Saori; Kawada, Yuta; Hashimoto, Hisako; Yamaguchi, Masahiko
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 93
• Pages of publication: 13580 - 13583
• a: 9.1542 ± 0.0014 Å
• b: 16.965 ± 0.0015 Å
• c: 10.682 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1658.9 ± 0.4 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.2095
• Residual factor for significantly intense reflections: 0.1403
• Weighted residual factors for significantly intense reflections: 0.3766
• Weighted residual factors for all reflections included in the refinement: 0.4216
• Goodness-of-fit parameter for all reflections included in the refinement: 1.31
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No