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Information card for entry 7125250
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Coordinates | 7125250.cif |
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Original paper (by DOI) | HTML |
Formula | C21 H24 N2 O Si |
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Calculated formula | C21 H24 N2 O Si |
Title of publication | Palladium-catalyzed direct intermolecular silylation of remote unactivated C(sp<sup>3</sup>)-H bonds. |
Authors of publication | Pan, Jin-Long; Li, Quan-Zhe; Zhang, Ting-Yu; Hou, Si-Hua; Kang, Jun-Cheng; Zhang, Shu-Yu |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2016 |
Journal volume | 52 |
Journal issue | 89 |
Pages of publication | 13151 - 13154 |
a | 10.08 ± 0.0003 Å |
b | 11.8813 ± 0.0004 Å |
c | 16.5509 ± 0.0006 Å |
α | 88.653 ± 0.002° |
β | 86.499 ± 0.002° |
γ | 89.381 ± 0.002° |
Cell volume | 1977.86 ± 0.11 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0715 |
Residual factor for significantly intense reflections | 0.0536 |
Weighted residual factors for significantly intense reflections | 0.1413 |
Weighted residual factors for all reflections included in the refinement | 0.1518 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.033 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7125250.html
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