Information card for entry 7125250

Structure parameters

• Formula: C21 H24 N2 O Si
• Calculated formula: C21 H24 N2 O Si
• Title of publication: Palladium-catalyzed direct intermolecular silylation of remote unactivated C(sp³)-H bonds.
• Authors of publication: Pan, Jin-Long; Li, Quan-Zhe; Zhang, Ting-Yu; Hou, Si-Hua; Kang, Jun-Cheng; Zhang, Shu-Yu
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 89
• Pages of publication: 13151 - 13154
• a: 10.08 ± 0.0003 Å
• b: 11.8813 ± 0.0004 Å
• c: 16.5509 ± 0.0006 Å
• α: 88.653 ± 0.002°
• β: 86.499 ± 0.002°
• γ: 89.381 ± 0.002°
• Cell volume: 1977.86 ± 0.11 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0715
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.1413
• Weighted residual factors for all reflections included in the refinement: 0.1518
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No