Information card for entry 7125251

Structure parameters

• Formula: C20 H30 N2 O Si2
• Calculated formula: C20 H30 N2 O Si2
• Title of publication: Palladium-catalyzed direct intermolecular silylation of remote unactivated C(sp³)-H bonds.
• Authors of publication: Pan, Jin-Long; Li, Quan-Zhe; Zhang, Ting-Yu; Hou, Si-Hua; Kang, Jun-Cheng; Zhang, Shu-Yu
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 89
• Pages of publication: 13151 - 13154
• a: 17.5738 ± 0.0008 Å
• b: 10.3894 ± 0.0004 Å
• c: 12.0069 ± 0.0005 Å
• α: 90°
• β: 100.934 ± 0.002°
• γ: 90°
• Cell volume: 2152.44 ± 0.16 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0495
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.1225
• Weighted residual factors for all reflections included in the refinement: 0.1337
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No