Information card for entry 7125252

Structure parameters

• Formula: C26 H29 N3 O3 Si
• Calculated formula: C26 H29 N3 O3 Si
• Title of publication: Palladium-catalyzed direct intermolecular silylation of remote unactivated C(sp³)-H bonds.
• Authors of publication: Pan, Jin-Long; Li, Quan-Zhe; Zhang, Ting-Yu; Hou, Si-Hua; Kang, Jun-Cheng; Zhang, Shu-Yu
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 89
• Pages of publication: 13151 - 13154
• a: 40.8407 ± 0.0009 Å
• b: 11.72 ± 0.0003 Å
• c: 10.659 ± 0.0002 Å
• α: 90°
• β: 102.731 ± 0.001°
• γ: 90°
• Cell volume: 4976.53 ± 0.19 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0521
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.1094
• Weighted residual factors for all reflections included in the refinement: 0.113
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No