Information card for entry 7125258

Structure parameters

• Formula: C24 H36 O2 P2 Pd S
• Calculated formula: C24 H36 O2 P2 Pd S
• Title of publication: Highly efficient reduction of carbon dioxide with a borane catalyzed by bis(phosphinite) pincer ligated palladium thiolate complexes.
• Authors of publication: Ma, Qiang-Qiang; Liu, Ting; Li, Shujun; Zhang, Jie; Chen, Xuenian; Guan, Hairong
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 99
• Pages of publication: 14262 - 14265
• a: 8.7065 ± 0.0015 Å
• b: 11.0937 ± 0.0019 Å
• c: 15.13 ± 0.003 Å
• α: 73.3056 ± 0.0017°
• β: 80.9582 ± 0.0019°
• γ: 74.899 ± 0.0018°
• Cell volume: 1346.1 ± 0.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0286
• Residual factor for significantly intense reflections: 0.0235
• Weighted residual factors for significantly intense reflections: 0.0657
• Weighted residual factors for all reflections included in the refinement: 0.0757
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No